HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1-(2-pyridinyl)-1-ethanone hydrobromide → HCID 18613913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1-(2-pyridinyl)-1-ethanone hydrobromide | HCID 2776231 | — |
| Reactant | Methyl 4-carbamothioylbenzoate | HCID 11401319 | — |
| Product | HCID 18613913 | HCID 18613913 | 80% |
Reaction Steps
In the same manner as in Example 28, methyl 4-thiocarbamoylbenzoate was reacted with 2-bromoacetylpyridine hydrobromide to obtain methyl 4-[4-(2-pyridyl)-2-thiazolyl]benzoate hydrobromide. The product was recrystallized from ethanol. Yield: 80%. Pale yellow prisms. Melting point: 243 to 244° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-d81fd3f63a934453b2ec38cdb41fd618 |
| Source note | uspto-grants-2003_04 |