HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1-(pentafluorophenyl)ethan-1-one → HCID 18613824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1-(pentafluorophenyl)ethan-1-one | HCID 2775963 | — |
| Reactant | Methyl 4-carbamothioylbenzoate | HCID 11401319 | — |
| Product | HCID 18613824 | HCID 18613824 | 60% |
Reaction Steps
In the same manner as in Example 28, methyl 4-thiocarbamoylbenzoate was reacted with 2,3,4,5,6-pentafluorophenacyl bromide to obtain methyl 4-[4-(2,3,4,5,6-pentafluorophenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 60%. Pale yellow prisms. Melting point: 141 to 142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-7913757938084c16b952af0405113729 |
| Source note | uspto-grants-2003_04 |