HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-3'-chloroacetophenone → HCID 18613875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-3'-chloroacetophenone | HCID 38738 | — |
| Reactant | Methyl 4-carbamothioylbenzoate | HCID 11401319 | — |
| Product | HCID 18613875 | HCID 18613875 | 72% |
Reaction Steps
In the same manner as in Example 28, methyl 4-thiocarbamoylbenzoate was reacted with 3-chlorophenacyl bromide to obtain methyl 4-[4-(3-chlorophenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 72%. Pale yellow prisms. Melting point: 150 to 151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-fd2201c6ac3e40c9b0a6084c51af2514 |
| Source note | uspto-grants-2003_04 |