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HRID1264943

反应详情

EQUATION

反应方程式

HRID 1264943 的结构方程式

REACTANTS

反应物

2
结构：O=C(CBr)c1ccc(C(F)(F)F)cc1
HCID321979

4-(Trifluoromethyl)phenacyl bromide

C9H6BrF3O

结构：COC(=O)c1cccc(C(N)=S)c1
HCID23279244

Methyl 3-carbamothioylbenzoate

C9H9NO2S

PRODUCTS

生成物

1
结构：COC(=O)c1cccc(-c2nc(-c3ccc(C(F)(F)F)cc3)cs2)c1
HCID18613836

未命名化合物

收率 74%

PROCEDURE

实验过程

In the same manner as in Example 28, methyl 3-thiocarbamoylbenzoate was reacted with 4-trifluoromethylphenacyl bromide to obtain methyl 3-[4-(4- trifluoromethylphenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 74%. Colorless prisms. Melting point: 142 to 143° C.