HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1-[3-(trifluoromethyl)phenyl]ethan-1-one → HCID 18613861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1-[3-(trifluoromethyl)phenyl]ethan-1-one | HCID 2778386 | — |
| Reactant | Methyl 3-carbamothioylbenzoate | HCID 23279244 | — |
| Product | HCID 18613861 | HCID 18613861 | 72% |
Reaction Steps
In the same manner as in Example 28, methyl 3-thiocarbamoylbenzoate was reacted with 3-trifluoromethylphenacyl bromide to obtain methyl 3-[4-(3-trifluoromethylphenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 72%. Colorless prisms. Melting point: 105 to 106° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-51771fffc8214589b284eb6f1a6ac3a9 |
| Source note | uspto-grants-2003_04 |