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HRID1264946

反应详情

EQUATION

反应方程式

HRID 1264946 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(C(=O)CBr)cc1
HCID4965

Bromomethyl 4-methoxyphenyl ketone

C9H9BrO2

结构：COC(=O)c1cccc(C(N)=S)c1
HCID23279244

Methyl 3-carbamothioylbenzoate

C9H9NO2S

PRODUCTS

生成物

1
结构：COC(=O)c1cccc(-c2nc(-c3ccc(OC)cc3)cs2)c1
HCID18613878

未命名化合物

收率 74%

PROCEDURE

实验过程

In the same manner as in Example 28, methyl 3-thiocarbamoylbenzoate was reacted with 4-methoxyphenacyl bromide to obtain methyl 3-[4-(4-methoxyphenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 74%. Pale yellow prisms. Melting point: 108 to 109° C.