HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethyl 4-methoxyphenyl ketone → HCID 18613878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethyl 4-methoxyphenyl ketone | HCID 4965 | — |
| Reactant | Methyl 3-carbamothioylbenzoate | HCID 23279244 | — |
| Product | HCID 18613878 | HCID 18613878 | 74% |
Reaction Steps
In the same manner as in Example 28, methyl 3-thiocarbamoylbenzoate was reacted with 4-methoxyphenacyl bromide to obtain methyl 3-[4-(4-methoxyphenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 74%. Pale yellow prisms. Melting point: 108 to 109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-1ba504dbe30c473d856200cc43878cd4 |
| Source note | uspto-grants-2003_04 |