HRID1264948

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID18613869

2-Bromo-1-(2,5-dimethylfuran-3-yl)ethan-1-one

C8H9BrO2

HCID18613909

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)c1cccc(-c2nc(-c3cc(C)oc3C)cs2)c1

HCID18613843

未命名化合物

收率 16%

PROCEDURE

实验过程

In the same manner as in Example 28, ethyl 3-thiocarbamoylbenzoate was reacted with 3-bromoacetyl-2,5-dimethylfuran to obtain ethyl 3-[4-(2,5-dimethyl-3-furyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 16%, Pale yellow prisms. Melting point: 100 to 101° C.