huagongshe.com
HRID1264949

反应详情

EQUATION

反应方程式

HRID 1264949 的结构方程式

REACTANTS

反应物

2
结构：O=C(CBr)c1cccc(OC(F)(F)F)c1
HCID2778687

2-Bromo-3'-trifluoromethoxyacetophenone

C9H6BrF3O2

结构：COC(=O)c1cccc(C(N)=S)c1
HCID23279244

Methyl 3-carbamothioylbenzoate

C9H9NO2S

PRODUCTS

生成物

1
结构：COC(=O)c1cccc(-c2nc(-c3cccc(OC(F)(F)F)c3)cs2)c1
HCID18613812

未命名化合物

收率 34%

PROCEDURE

实验过程

In the same manner as in Example 28, methyl 3-thiocarbamoylbenzoate was reacted with 3-trifluoromethoxyphenacyl bromide to obtain methyl 3-[4-(3-trifluoromethoxyphenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 34%. Colorless prisms. Melting point: 84 to 85° C.