HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenacyl bromide → HCID 18613905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenacyl bromide | HCID 7454 | — |
| Reactant | Methyl 4-carbamothioylbenzoate | HCID 11401319 | — |
| Product | HCID 18613905 | HCID 18613905 | 73% |
Reaction Steps
In the same manner as in Example 74, methyl 4-thiocarbamoylbenzoate was reacted with 4-bromophenacyl bromide to obtain methyl 4-[4-(4-bromophenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 73%. Colorless prisms. Melting point: 206 to 207° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-cc6092ac34104869bcb4eb3ecc8dc4a7 |
| Source note | uspto-grants-2003_04 |