HRID1264951

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11401319

Methyl 4-carbamothioylbenzoate

C9H9NO2S

HCID18613869

2-Bromo-1-(2,5-dimethylfuran-3-yl)ethan-1-one

C8H9BrO2

PRODUCTS

生成物

结构：COC(=O)c1ccc(-c2nc(-c3cc(C)oc3C)cs2)cc1

HCID18613829

未命名化合物

收率 36%

PROCEDURE

实验过程

In the same manner as in Example 74, methyl 4-thiocarbamoylbenzoate was reacted with 3-bromoacetyl-2,5-dimethylfuran to obtain methyl 4-[4-(2,5-dimethyl-3-furyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 36%. Pale yellow prisms. Melting point: 103 to 105° C.