HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanone, 2-bromo-1-(2,5-dimethyl-3-thienyl)- → HCID 18613912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanone, 2-bromo-1-(2,5-dimethyl-3-thienyl)- | HCID 11241770 | — |
| Reactant | Methyl 4-carbamothioylbenzoate | HCID 11401319 | — |
| Product | HCID 18613912 | HCID 18613912 | 64% |
Reaction Steps
In the same manner as in Example 74, methyl 4-thiocarbamoylbenzoate was reacted with 3-bromoacetyl-2,5-dimethylthiophene to obtain methyl 4-[4-(2,5-dimethyl-3-thienyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 64%. Pale yellow pritsms. Melting point: 109 to 110° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-23fe72b46c964f6abe8f4998f3a40034 |
| Source note | uspto-grants-2003_04 |