HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-carbamothioylbenzoate → HCID 18613879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-carbamothioylbenzoate | HCID 11401319 | — |
| Reactant | HCID 18521789 | HCID 18521789 | — |
| Product | HCID 18613879 | HCID 18613879 | 74% |
Reaction Steps
In the same manner as in Example 74, methyl 4-thiocarbamoylbenzoate was reacted with 3-bromoacetyl-2,5-dichlorothiophene to obtain methyl 4-[4-(2,5-dichloro-3-thienyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 74%. Pale yellow prisms. Melting point: 149 to 150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-d60062fb682445f6b1b00f998d4fdf51 |
| Source note | uspto-grants-2003_04 |