Phosphorisocyanatidic acid, diethyl ester → HCID 22397376, compound

HRID 1265099Notes

Reaction equation

HRID 1265099 reaction equation
[CH2:1]([O:3][P:4]([N:9]=[C:10]=[O:11])([O:6][CH2:7][CH3:8])=[O:5])[CH3:2].[NH2:12][CH2:13][CH2:14][N:15]1[C:23]2[C:22]([CH3:24])=[C:21]([CH3:25])[N:20]=[C:19]([NH2:26])[C:18]=2[N:17]=[C:16]1[CH3:27]>>[NH2:26][C:19]1[C:18]2[N:17]=[C:16]([CH3:27])[N:15]([CH2:14][CH2:13][NH:12][C:10]([NH:9][P:4]([O:6][CH2:7][CH3:8])([O:3][CH2:1][CH3:2])=[O:5])=[O:11])[C:23]=2[C:22]([CH3:24])=[C:21]([CH3:25])[N:20]=1

Participants

3

Reactant 2

HCID 580184Phosphorisocyanatidic acid, diethyl esterHCID 219738201-(2-aminoethyl)-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine

Product 1

HCID 22397376HCID 22397376, compound

Procedure

Using the method of Examples 118-133, diethoxyphosphinyl isocyanate was reacted with 1-(2-aminoethyl)-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The observed accurate mass was 399.1926.

Sources & evidence

ORD record
ord-4a2f6eca3e484dada984ac74113e34c7
Source dataset
uspto-grants-2003_04
Patent number
US06545017B1

Reaction notes

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