Phosphorisocyanatidic acid, diethyl ester → diethyl{[2-(4-amino-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-1-yl)ethyl]amino}carbonylamidophosphate

Participants

Role	Name	HCID	Charge
Reactant	Phosphorisocyanatidic acid, diethyl ester	HCID 580184	—
Reactant	1-(2-aminoethyl)-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine	HCID 21973820	—
Product	diethyl{[2-(4-amino-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-1-yl)ethyl]amino}carbonylamidophosphate	HCID 22397376	—

Reaction Steps

Using the method of Examples 118-133, diethoxyphosphinyl isocyanate was reacted with 1-(2-aminoethyl)-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The observed accurate mass was 399.1926.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06545017B1
Source dataset	uspto-grants-2003_04
ORD ID	ord-4a2f6eca3e484dada984ac74113e34c7
Source note	uspto-grants-2003_04