HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[3-(2-bromoacetyl)phenyl]methanesulfonamide → (+/-)-N-[3-(2-bromo-1-hydroxyethyl)phenyl]methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[3-(2-bromoacetyl)phenyl]methanesulfonamide | HCID 11346858 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | (+/-)-N-[3-(2-bromo-1-hydroxyethyl)phenyl]methanesulfonamide | HCID 18615063 | — |
Reaction Steps
The above-identified compound (50.76 g) was obtained by processing Intermediate 14 (45 g) through reaction and after-treatment in accordance with the procedures of synthesis of Intermediate 41. Rf=0.27 (methanol/chloroform of 1/10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545053B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-3e5457bc3184484582942ecbb1c89b3d |
| Source note | uspto-grants-2003_04 |