HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine chloride → 5-Chloro-4-iodo-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine chloride | HCID 24640 | — |
| Reactant | 5-Chloro-2-nitroaniline | HCID 74218 | — |
| Solvent | Sodium Diacetate | HCID 23662384 | — |
| Product | 5-Chloro-4-iodo-2-nitroaniline | HCID 22317548 | — |
Reaction Steps
The title compound was prepared from 5-chloro-2-nitroaniline by iodination with iodine monochloride in HOAc/NaOAc according to the general procedure A (80° C.). Obtained as an orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-dfd014f423cb4505b930825cdb77fbac |
| Source note | uspto-grants-2003_04 |