HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 69688164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Azetidine | HCID 10422 | — |
| Reactant | (5-Chloro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester | HCID 69489376 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 69688164 | HCID 69688164 | — |
Reaction Steps
The title compound was prepared from (5-chloro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert.-butyl ester (Example B5), azetidine and Et3N in DMSO at 23° C. according to the general procedure C. Obtained as a yellow solid (6.925 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-aa2ec652680f43ec8f580d3d2a7a0e6c |
| Source note | uspto-grants-2003_04 |