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HRID1265516

反应详情

EQUATION

反应方程式

HRID 1265516 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：C1CNC1
HCID10422

Azetidine

C3H7N

结构：CC(C)(C)OC(=O)Nc1cc(Cl)c(C(F)(F)F)cc1[N+](=O)[O-]
HCID69489376

1,1-Dimethylethyl N-[5-chloro-2-nitro-4-(trifluoromethyl)phenyl]carbamate

C12H12ClF3N2O4

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Nc1cc(N2CCC2)c(C(F)(F)F)cc1[N+](=O)[O-]
HCID69688164

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

The title compound was prepared from (5-chloro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert.-butyl ester (Example B5), azetidine and Et3N in DMSO at 23° C. according to the general procedure C. Obtained as a yellow solid (6.925 g).