HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → HCID 69688527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | HCID 86586794 | HCID 86586794 | — |
| Product | HCID 69688527 | HCID 69688527 | — |
Reaction Steps
The title compound was prepared from [4-chloro-5-(cyclopropyl-methyl-amino)-2-nitro-phenyl]-carbamic acid tert.-butyl ester (Example C9) (3.2 g, 9.36 mmol) by reduction with SnCl2.2H2O according to the general procedure J (method b). Obtained as brown solid (2.00 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-be81bfd4ade34cb4b430dfe45d13660b |
| Source note | uspto-grants-2003_04 |