HCID 69688430, compound → HCID 69688803, compound

HRID 1265558Notes

Reaction equation

HRID 1265558 reaction equation
[C:1]([O:5][C:6](=[O:22])[NH:7][C:8]1[CH:13]=[C:12]([N:14]2[CH2:17][CH2:16][CH2:15]2)[C:11]([Cl:18])=[CH:10][C:9]=1[N+:19]([O-])=O)([CH3:4])([CH3:3])[CH3:2]>[Pt]>[C:1]([O:5][C:6](=[O:22])[NH:7][C:8]1[CH:13]=[C:12]([N:14]2[CH2:17][CH2:16][CH2:15]2)[C:11]([Cl:18])=[CH:10][C:9]=1[NH2:19])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 1

HCID 69688430HCID 69688430, compound

Product 1

HCID 69688803HCID 69688803, compound

Reagents, catalysts & solvents 1

HCID 23939PlatinumCatalyst

Procedure

The title compound was prepared from (5-azetidin-1-yl-4-chloro-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example C14) by hydrogenation with 5% Pt/C according to the general procedure J (method a). Obtained as a white solid (3.664 g).

Sources & evidence

ORD record
ord-696590d0656747908d53007dbe17e6b4
Source dataset
uspto-grants-2003_04
Patent number
US06544985B2

Reaction notes

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