HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Dimethylamino-2'-fluoro-5-nitro-biphenyl-4-yl)-carbamic acid tert-butyl ester → HCID 69489440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Dimethylamino-2'-fluoro-5-nitro-biphenyl-4-yl)-carbamic acid tert-butyl ester | HCID 69489429 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 69489440 | HCID 69489440 | — |
Reaction Steps
The title compound was prepared from (2-dimethylamino-2′-fluoro-5-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example C18) (4.54 g, 12.1 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a light brown solid (3.324 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-7e9dc96e1dfe496fb4bee129860bb76c |
| Source note | uspto-grants-2003_04 |