HCID 69688169, compound → HCID 69688306, compound

HRID 1265564Notes

Reaction equation

HRID 1265564 reaction equation
[C:1]([O:5][C:6](=[O:21])[NH:7][C:8]1[CH:13]=[C:12]([N:14]([CH3:16])[CH3:15])[C:11]([CH3:17])=[CH:10][C:9]=1[N+:18]([O-])=O)([CH3:4])([CH3:3])[CH3:2]>[Pd]>[C:1]([O:5][C:6](=[O:21])[NH:7][C:8]1[CH:13]=[C:12]([N:14]([CH3:15])[CH3:16])[C:11]([CH3:17])=[CH:10][C:9]=1[NH2:18])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 1

HCID 69688169HCID 69688169, compound

Product 1

HCID 69688306HCID 69688306, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

The title compound was prepared from (5-dimethylamino-4-methyl-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example C19) (3.22 g, 10.9 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a gray solid (2.05 g, 58%).

Sources & evidence

ORD record
ord-7e86d1ce920840119878ca8f4e20f684
Source dataset
uspto-grants-2003_04
Patent number
US06544985B2

Reaction notes

Loading…