HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69688169, compound → (2-Amino-5-dimethylamino-4-methyl-phenyl)-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69688169 | HCID 69688169 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | (2-Amino-5-dimethylamino-4-methyl-phenyl)-carbamic acid tert-butyl ester | HCID 69688306 | — |
Reaction Steps
The title compound was prepared from (5-dimethylamino-4-methyl-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example C19) (3.22 g, 10.9 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a gray solid (2.05 g, 58%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-7e86d1ce920840119878ca8f4e20f684 |
| Source note | uspto-grants-2003_04 |