HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69688409, compound → Carbamic acid,[2-amino-5-(ethylmethylamino)-4-methylphenyl]-,1,1-dimethylethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69688409 | HCID 69688409 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Carbamic acid,[2-amino-5-(ethylmethylamino)-4-methylphenyl]-,1,1-dimethylethyl ester | HCID 69688364 | — |
Reaction Steps
The title compound was prepared from [5-(ethyl-methyl-amino)-4-methyl-2-nitro-phenyl]-carbamic acid tert-butyl ester (Example C22) (3.28 g, 10.6 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a purple solid (2.94 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-c540f50ef1904be7b3d8cdf5d49f2116 |
| Source note | uspto-grants-2003_04 |