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HRID1265641

反应详情

EQUATION

反应方程式

HRID 1265641 的结构方程式

REACTANTS

反应物

2
结构：O=C(OC(=O)C(F)(F)F)C(F)(F)F
HCID9845

Trifluoroacetic anhydride

C4F6O3

结构：CC(C)(C)OC(=O)CC(=O)c1cccc(-n2ccnn2)c1
HCID69687599

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)OC(=O)C=C(c2cccc(-n3ccnn3)c2)O1
HCID18548744

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O.O=C(O)C(F)(F)F
溶剂HCID86586799

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 3-oxo-3-(3-[1,2,3]triazol-1-yl -phenyl)-propionic acid tert.-butyl ester (Example K23) by stirring in TFA/acetone with TFAA according to general procedure L (method b). Obtained as a beige solid (7.80 g).