HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18613404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86586802 | HCID 86586802 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18613404 | HCID 18613404 | — |
Reaction Steps
The title compound was prepared from {2-[3-(3-cyano-phenyl)-3-oxo-propionyl-amino]-5-dimethylamino-4-phenylethynyl-phenyl}-carbamic acid tert.-butyl ester (Example M4) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as an orange solid (65 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-a761b1f10ce145e6b031e2a5e1630df6 |
| Source note | uspto-grants-2003_04 |