HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18613294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86586842 | HCID 86586842 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18613294 | HCID 18613294 | — |
Reaction Steps
The title compound was prepared from {5-azetidin-1-yl-4-chloro-2-[3-(2-cyano-pyridin-4-yl)-3-oxo-propionylamino]-phenyl}-carbamic acid tert. -butyl ester (Example M50) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as an orange solid (66 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-50bf607ab9a94c61af86ca364fc9730c |
| Source note | uspto-grants-2003_04 |