HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18613410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86586918 | HCID 86586918 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18613410 | HCID 18613410 | — |
Reaction Steps
The title compound was prepared from {2-[3-(3-Cyano-phenyl)-3-oxo-propionyl-amino]-4-dimethylamino-5-methyl-phenyl}-carbamic acid tert-butyl ester (Example M76) (0.24 g, 0.55 mmol) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as a pale yellow solid (114 mg, 59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-de8c677a3b0542b98a9c2593a42f6469 |
| Source note | uspto-grants-2003_04 |