HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18613474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86586919 | HCID 86586919 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18613474 | HCID 18613474 | — |
Reaction Steps
The title compound was prepared from {5-cyano-2-[3-(3-cyano-phenyl)-3-oxo-propionylamino]-4-dimethylamino-phenyl}-carbamic acid tert-butyl ester (Example M78) (0.28 g, 0.63 mmol) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as a yellow solid (36 mg, 59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-46df6f3fefd74961a6da986a9db5044d |
| Source note | uspto-grants-2003_04 |