HCID 69701971, compound → HCID 69701319, compound

Participants

Reaction Steps

This known compound was prepared from 3,4,6,7-tetrahydro-2H-[1,4]diazepino[6,7,1-hi]indol-1-one (Example 41) according to the general procedure of Hester et al. and references cited therein (Hester et al., J. Med. Chem. 13, 827 (1970)): 1H NMR (DMSO-d6) δ 3.52-3.56 (m, 2H), 4.31-4.36 (m, 2H), 6.53 (d, 1H, J=3.0 Hz), 7.11 (t, 1H, J=6.0 Hz), 7.38 (d, 1H, J=3.0 Hz), 7.70 (d, 1H, J=6.0 Hz), 7.80 (d, 1H, J=6.0 Hz), 8.30 (bs, 1H). LRMS (M+) 186. Anal. (C11H10N2O.0.05 H2O) C, H, N.

Provenance & Evidence