HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 69701208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 69700490 | HCID 69700490 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 69701208 | HCID 69701208 | — |
Reaction Steps
This compound was prepared by reacting 500 mg (1.7 mmol) of alcohol 58a, suspended in 25 mL of acetonitrile with 4 equivalents of thionyl chloride. After complete conversion as determined by HPLC analysis the reaction was concentrated in vacuo and the crude benzylchloride was without further purification. HPLC Rt=3.060 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548494B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-bb7d1793d40848209e5aacd24b776c17 |
| Source note | uspto-grants-2003_04 |