HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 137178912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Reactant | HCID 54540895 | HCID 54540895 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 137178912 | HCID 137178912 | — |
Reaction Steps
NaNO2 (0.35 g, 5 mmol) was added to a suspension of the product of step (b) above, (0.98 g, 4 mmol), in 3N HCl (20 mL), and H2O (20 mL). The slurry was stirred for 3 hours, filtered, washed with water, air dried to give the title compound. MS(ES) m/e 277 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548503B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-156efc7ce94c42eea15a81d4f7e6ceab |
| Source note | uspto-grants-2003_04 |