HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetaldehyde → HCID 18549631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetaldehyde | HCID 998 | — |
| Reactant | 1,3-Benzodioxol-5-amine | HCID 84310 | — |
| Reactant | Tetronic acid | HCID 521261 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18549631 | HCID 18549631 | — |
Reaction Steps
10 mmol of phenylacetaldehyde and 10 mmol of tetronic acid are added to 10 mmol of 3,4-methylenedioxyaniline dissolved in ethanol, then the reaction mixture is heated at reflux for the night. After returning to ambient temperature, the precipitate obtained is filtered and then washed with ethanol to yield the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548515B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-41ac18f1fb4141eabd4549bc86015f8c |
| Source note | uspto-grants-2003_04 |