HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Dimethylaminobutylamine → 5-[3-(4-Dimethylamino-butyl)-ureido]-3-(2,3,6-trifluoro-4-methyl-benzyloxy) isothiazole-4-carboxylic acid amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Dimethylaminobutylamine | HCID 77063 | — |
| Reactant | [4-Carbamoyl-3-(2,3,6-trifluoro-4-methyl-benzyloxy)-isothiazol-5-yl]-carbamic acid phenyl ester | HCID 54053016 | — |
| Product | 5-[3-(4-Dimethylamino-butyl)-ureido]-3-(2,3,6-trifluoro-4-methyl-benzyloxy) isothiazole-4-carboxylic acid amide | HCID 10366941 | — |
Reaction Steps
The title compound was prepared from [4-carbamoyl-3-(2,3,6-trifluoro-4-methyl-benzyloxy)-isothiazol-5-yl]-carbamic acid phenyl ester and N,N-dimethyl-butane-1,4-diamine by the procedure analogous to Example 1. MS (APCl, m/z): 460 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548526B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-7c35d492d6f54c54902aef2e14f3beb8 |
| Source note | uspto-grants-2003_04 |