Benzaldehyde → Phenyl trans-Styryl Sulfone
Reaction equation
[C:1]1([S:7]([CH2:10][C:11](O)=O)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(=O)[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:1]1([S:7](/[CH:10]=[CH:11]/[C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Participants
3
Procedure
A solution of phenyl sulfonylacetic acid (0.01 mol) and benzaldehyde (0.01 mol) was subjected to the Procedure 1. The title compound was obtained in 68-72% yield.
Sources & evidence
- ORD record
- ord-83ec8352a0a0489ab4cef0d2f12d099b
- Source dataset
- uspto-grants-2003_04
- Patent number
- US06548553B2
Reaction notes
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