4-Chlorobenzaldehyde → HCID 11162162, compound

HRID 1266483Notes

Reaction equation

[CH2:1]([S:8]([CH2:11][C:12](O)=O)(=[O:10])=[O:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl:15][C:16]1[CH:23]=[CH:22][C:19](C=O)=[CH:18][CH:17]=1>>[CH2:1]([S:8](/[CH:11]=[CH:12]/[C:19]1[CH:22]=[CH:23][C:16]([Cl:15])=[CH:17][CH:18]=1)(=[O:10])=[O:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 77264-Chlorobenzaldehyde

HCID 308062Phenylmethanesulfonyl-acetic acid

Product 1

HCID 11162162HCID 11162162, compoundYield 78%

Procedure

A solution of benzyl sulfonylacetic acid (0.01 mol) and 4-chlorobenzaldehyde (0.01 mol) was subjected to Procedure 1. The title compound was obtained in 78% yield.

Sources & evidence

ORD record: ord-f2cbc6bf6ca14a3d8ded4e62742adc54
Source dataset: uspto-grants-2003_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06548553B2

Reaction notes

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