HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 74990038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 76502387 | HCID 76502387 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 74990038 | HCID 74990038 | 94% |
Reaction Steps
To a solution of quinoxaline-2-carboxylic acid {1-[4-(3-fluoro-3-methyl-butyl)-5-oxo-tetrahydro-furan-2-yl]-2-phenyl-ethyl}-amide (220 mg, 0.489 mmol) in methanol (5 mL) was added excess hydrazine (0.500 mL) and stirred for 18 hours. The reaction was concentrated to give the title compound (222 mg, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548671B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-8d2f8e1f1e924c33853eb0113b5fdf1f |
| Source note | uspto-grants-2003_04 |