Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | M-Xylene | HCID 7929 | — |
| Reactant | Isobutyryl chloride | HCID 62325 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 583728 | HCID 583728 | — |
Reaction Steps
Aluminium chloride (28.0 g, 0.21 mole) was suspended in 200 ml of anhydrous dichloromethane and cooled to 0° C. A solution of m-xylene (21.2 g, 0.2 mole) and isobutyryl chloride (21.3 g, 0.20 mole) in 50 ml of anhydrous dichloromethane was slowly added to this suspension. After the addition was completed, the reaction mixture was stirred at 0° C. for 1 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06548710B2 |
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| Source dataset | uspto-grants-2003_04 |
|---|
| ORD ID | ord-ddca7330a19648a8b4435264c1ec2752 |
|---|
| Source note | uspto-grants-2003_04 |
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