HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 22317920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 5-Chloro-2-nitro-4-(trifluoromethyl)aniline | HCID 2773813 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 22317920 | HCID 22317920 | — |
Reaction Steps
The title compound was prepared from 5-chloro-2-nitro-4-trifluoromethyl-phenylamine [CAS-No. 35375-74-7] (4.61 g, 19.2 mmol) and KOH (2.78 g, 42.2 mmol) in MeOH (20 mL) and DMSO (40 mL) according to the general procedure E. Obtained as a yellow solid (4.18 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-08db82a560ce4e2bbf623c741520db92 |
| Source note | uspto-grants-2003_04 |