HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → (2-Amino-5-thiomorpholin-4-yl-4-trifluoromethyl-phenyl)-carbamic acid tert.-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | HCID 69781296 | HCID 69781296 | — |
| Product | (2-Amino-5-thiomorpholin-4-yl-4-trifluoromethyl-phenyl)-carbamic acid tert.-butyl ester | HCID 69780198 | — |
Reaction Steps
The title compound was prepared from (2-nitro-5-thiomorpholin-4-yl-4-trifluoromethyl-phenyl)-carbamic acid tert.-butyl ester (Example B2) (1.2 g, 2.95 mmol) by reduction with SnCl2.2H2O according to the general procedure J (method b). Obtained as a yellow solid (978 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-70adc6cbc2e74bdfbd5dad2c29e07eff |
| Source note | uspto-grants-2003_04 |