HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2,2-Dimethyl-6-oxo-6H-[1,3]dioxin-4-yl)-benzonitrile → HCID 86586973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2,2-Dimethyl-6-oxo-6H-[1,3]dioxin-4-yl)-benzonitrile | HCID 11736337 | — |
| Reactant | HCID 69780025 | HCID 69780025 | — |
| Product | HCID 86586973 | HCID 86586973 | — |
Reaction Steps
The title compound was prepared from [2-amino-4-(2-tert.-butyl-pyrrol-1-yl)-5-methoxy-phenyl]-carbamic acid tert.-butyl ester (Example J5) (89 mg, 0.25 mmol) and 3-(2,2-dimethyl-6-oxo-6H-[1,3]dioxin-4-yl)-benzonitrile (Example L1) (63 mg, 0.275 mmol) according to the general procedure M. Obtained as an off-white solid (72 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-14992c1ce41647fe93abe6a151df1411 |
| Source note | uspto-grants-2003_04 |