HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(3-Imidazol-1-yl-phenyl)-2,2-dimethyl-[1,3]dioxin-4-one → HCID 86586975, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(3-Imidazol-1-yl-phenyl)-2,2-dimethyl-[1,3]dioxin-4-one | HCID 22224895 | — |
| Reactant | HCID 69781137 | HCID 69781137 | — |
| Product | HCID 86586975 | HCID 86586975 | — |
Reaction Steps
The title compound was prepared from (2-amino-5-cyanomethyl-4-iodo-phenyl)-carbamic acid tert.-butyl ester (Example J6) (363 mg, 0.973 mmol) and 6-(3-imidazol-1-yl-phenyl)-2,2-dimethyl-[1,3]dioxin-4-one (Example L3) (411 mg, 1.52 mmol) according to the general procedure M. Obtained as a yellow oil (523 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-f3fd74035f6447df843dc1c0cd799e3a |
| Source note | uspto-grants-2003_04 |