HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → HCID 23500559, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 9815732 | HCID 9815732 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23500559 | HCID 23500559 | — |
Reaction Steps
To a solution of the product of Example 11 in methylene chloride at 0° C. is added carbon tetrabromide and triphenylphosphine. The reaction is stirred for 2 hours and the solvent is removed under reduced pressure. The crude product is dissolved in an eluting solvent system and chromatographed to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06552052B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-0ce58ad626d94b07abee9280696ba581 |
| Source note | uspto-grants-2003_04 |