HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → Ethyl 2-(4,4,5,5,6,6,7,7,7-nonafluoroheptyl)-9-decenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | 8-Bromooct-1-ene | HCID 75907 | — |
| Reactant | 4,4,5,5,6,6,7,7,7-Nonafluoroheptyl iodide | HCID 12016774 | — |
| Product | Ethyl 2-(4,4,5,5,6,6,7,7,7-nonafluoroheptyl)-9-decenoate | HCID 22718049 | — |
Reaction Steps
Starting with the 1-iodo-4,4,5,5,6,6,7,7,7-nonafluoroheptane prepared in Example 1, diethyl malonate and 8-bromooct-1-ene, a procedure analogous to that as shown in Example 3, 4 or 5 was repeated to give ethyl 2-(4,4,5,5,6,6,7,7,7-nonafluoroheptyl)-9-decenoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06552069B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-7677d2d6dfbb43e78ee5372a0b5cde4b |
| Source note | uspto-grants-2003_04 |