HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54378998, compound → HCID 54526015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54378998 | HCID 54378998 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54526015 | HCID 54526015 | 87.9% |
Reaction Steps
340 mg of 6-benzyl-8-(methoxyimino)-2-methyl-2,6-diazaspiro[3,4]octane was dissolved in 10 ml of methanol and thereto 300 mg of 10% Pd-C was added. The resulting mixture was stirred for 2 hours at 50° C. under the pressure of hydrogen, filtered and concentrated under the reduced pressure to give 195 mg of the titled compound (yield: 85.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06552196B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-7af78abc1d1b48f0bec0f3a7594e0864 |
| Source note | uspto-grants-2003_04 |