Phenylboronic Acid → HCID 16125935, compound
Reaction equation
[C:1]1(B(O)O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl[C:11]1[CH:12]=[C:13]([CH:19]=[CH:20][N:21]=1)[C:14]([O:16][CH2:17][CH3:18])=[O:15]>>[C:1]1([C:11]2[CH:12]=[C:13]([CH:19]=[CH:20][N:21]=2)[C:14]([O:16][CH2:17][CH3:18])=[O:15])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Participants
3
Procedure
Phenylboronic acid (147 mg) and ethyl 2-chloroisonicotinate (200 mg) were treated in the same manner as in Preparation Example 1 to obtain the title compound.
Sources & evidence
- ORD record
- ord-4b63646aebe946e48b3e6d7267dc88ff
- Source dataset
- uspto-grants-2003_04
- Patent number
- US06552188B2
Reaction notes
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