HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinecarbonyl chloride, hydrochloride (1:1) → Hydrochloric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
| Reactant | 1-[[2-(3,4,5-Trimethoxyphenyl)pyridin-4-yl]-methyl]piperazine | HCID 12021155 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | N-nicotinoyl-N'-[[2-(3,4,5-trimethoxyphenyl)-pyridin-4-yl]methyl]piperazine | HCID 18546845 | — |
Reaction Steps
1-[[2-(3,4,5-Trimethoxyphenyl)pyridin-4-yl]methyl]-piperazine (103 mg) and nicotinic acid chloride hydrochloride (70 mg) were reacted in the same manner as in Example 46 to obtain the title compound as a hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06552188B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-2444bad2beab4b38a62f0209b0e231ee |
| Source note | uspto-grants-2003_04 |