Hydrochloric Acid → HCID 20287976, compound

HRID 126772Notes

Reaction equation

HRID 126772 reaction equation
[CH2:1]([O:3][C:4]1[C:5]2[N:6]([CH:14]=[C:15]([C:17]([O:19]CC)=[O:18])[N:16]=2)[C:7]2[C:12]([N:13]=1)=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH3:2].O.[OH-].[Na+].Cl>C(O)C>[CH2:1]([O:3][C:4]1[C:5]2[N:6]([CH:14]=[C:15]([C:17]([OH:19])=[O:18])[N:16]=2)[C:7]2[C:12]([N:13]=1)=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH3:2]

Participants

6

Reactant 4

HCID 313Hydrochloric AcidHCID 962WaterHCID 14798Sodium HydroxideHCID 20287982HCID 20287982, compound

Product 1

HCID 20287976HCID 20287976, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A suspension of 0.5 g of the product of Step B, 50 ml of water, 15 ml of ethanol and 8 ml of 1 N sodium hydroxide solution was stirred overnight to obtain a clear colorless solution which was acidified with concentrated hydrochloric acid. The mixture was filtered to obtain 4-ethoxy-imidazo-[1,2-a]-quinoxaline-2-carboxylic acid melting at 220°-222° C.

Workup

  1. customto obtain a clear colorless solution which
  2. filtrationThe mixture was filtered

Sources & evidence

ORD record
ord-9f1cd167462d4cbb885a9fa65c294349
Source dataset
uspto-grants-1981_03
Patent number
US04254123

Reaction notes

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