Tetrabutylammonium Fluoride → HCID 18542395, compound

Participants

Reaction Steps

A solution of tetrabutylammonium fluoride in THF (1M, 4.6 ml) was added to a solution of the product from step (c) (1.71 g) in THF (20 ml). The mixture was stirred at room temperature for 1 hour and evaporated to dryness. The residue was purified by flash chromatography eluting with 3% ethanol (EtOH) in dichloromethane (CH2Cl2) to give the product as a white solid. Yield 0.82 g.

Provenance & Evidence